bbc a history of britain revolutions part 2
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)
Ngày tải lên :
18/10/2013, 00:15
... concentration of an alkyl nitrite on the horizontal axis and peak area on the vertical
axis. e concentration of the analyte in a specimen is calculated using the calibration
curve.
Assessment and some ... cyanide to inactivate it [1]. Alkyl nitrites also show a coronary artery-di-
lating e ect, and had been, therefore, used for the treatment of angina pectoris many years ago
[2] ; the pharmacological ... rats. J Pharm Sci
74:780–7 82
10) Kielbasa WB, Bauer JA, Fung HL (1999) Analysis of isobutyl nitrite inhalant in rat and human blood: application
for pharmacokinetic investigations. J Chromatogr...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)
Ngày tải lên :
18/10/2013, 00:15
... construct a cali-
bration curve for DAEMS consisting of peak area ratio of DAEMS to IS on the vertical axis
and DAEMS concentration on the horizontal axis. A peak area ratio obtained from a test ... chromato-
gram; (b) an EI mass spectrum of DAEMS; (c) a CI mass spectrum of DAEMS.
⊡ Figure 2. 2
620 VX and its decomposition products
Reagent and their preparation
ã A 10-mg aliquot of EMPA (Aldrich, ... electrospray and atmospheric
pressure chemical ionization. J Chromatogr A 794 :23 3 24 4
12) Kostiainen R, Bruins AP, Hakkinen VMA (1993) Identification of degradation products of some chemical warfare...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)
Ngày tải lên :
24/10/2013, 19:15
... Fast Blue BB salt. Eisei Kagaku 25 : 321 – 326
6) Matsunaga T, Nagatomo H, Narimatsu S et al. (1993) Studies on identification of cannabis seeds. I: Qualitative
and quantitative analysis of cannabinoids ... principal constituents by thin-layer and gas chromatographies. Chem Pharm Bull 16: 822 – 826
4) Yokoyama M, Okada Y, Suzuki K (19 92) Determination of cannabinoids in cannabis oil by capillary gas chroma-
tography. ...
value of ∆
9
-THC-11-oic acid in urine at 50 ng/mL by immunoassay and the identi able value
of the acid by mass spectral measurements at 15 ng/mL.
Cases of analysis [13]
Case 1: A 22 -year-old...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
Ngày tải lên :
24/10/2013, 19:15
... use can be mentioned. In a chronic opiate-dependent patient, several
grams of an opiate do occasionally not cause death.
Toxic and fatal concentrations
20 2 Morphine and its analogues
ã 5 mM Ammonium ... its analogues
8) Matsubara K, Fukushima S, Akane A et al. (19 92) Increased urinary morphine, codeine and tetrahydropapavero-
line in Parkinsonian patient undergoing L-3,4-dihydroxyphenylalanine ... recommendable for diagnosis of heroin use, because of its relatively long
half-life in the body [4].
For accurate diagnosis of a cause of death in an opiate poisoning case, the ratio of a free...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)
Ngày tải lên :
24/10/2013, 19:15
... (1996) A case of severe methemoglobinemia for a newborn baby caused by
well water. Jpn J Pediatr 49:1661–1665 (in Japanese)
4) Saito T, Takeichi S, Osawa M et al. (20 00) A case of fatal methemoglobinemia ... (1987) Cyanosis in infants caused by nitrates in well water. JAMA 25 7 :27 88 27 92
12) Fan AM, Steinberg VE (1996) Health implications of nitrate and nitrite in drinking water: an update on methe-
moglobinemia ... it causes cyanosis, headache, easy fatigability, respiratory and conciousness dis-
turbances and nally death. e fatal methemoglobinemia is rare, but fatal ones a er ingestion
of nitrate...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)
Ngày tải lên :
24/10/2013, 19:15
... 181, 1 82
MBDB 22 9, 23 4
MBTFA 371
MDA 62, 63, 22 9, 23 4
MDEA 22 9, 23 4
MDMA 62, 63, 21 2, 22 9,
23 4
MDN-5S 188
meclizine 315
meconium 12
medazepam 28 4, 28 5
medical accidents 395
medium-bore capillary ... 85
alkylated DNAs 85
alkylation 30
alkyl nitrites 153, 655
allobarbital 305, 308
allylesterase 624
allyxycarb 566
alminoprofen 325 , 330, 3 32
alprazolam 28 4, 28 5, 29 0
alternative specimens 9
Amanita neoovoidea ... neoovoidea 480
Amanita pantherina 469
Amanita phalloides 469
Amanita verna 469, 474
Amanita virosa 469, 473
amanitin 473, 477, 479
amido-type local anesthetic
385
1-amino-4- phenylbutane
173
2- amino-6-hydroxymethyl-
8-hydroxyquinazoline...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)
Ngày tải lên :
29/10/2013, 01:15
... mL/min.
l) A majority of basic drugs is adsorbed to the cation exchanger phase, and a minor part is
adsorbed to the non-polar phase. e latter part is desorbed and adsorbed again to the
cation exchanger ... 4 .2
shows mass spectra of the authentic cocaine, EME and BE a er derivatization.
Setting up of cuto values are very common in USA and Europe as a part of QC ( quality
control) and QA ( quality ... obtain a clean mass spectrum;
while at 20 0 ng/mL of BE in blood, a satisfactory mass spectrum can be obtained. For BE,
Metabolic pathways of cocaine.
⊡ Figure 4.4
Toxic and fatal concentrations
...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)
Ngày tải lên :
29/10/2013, 02:15
... horizontal axis and peak area ratio of pentazocine to IS in the
vertical axis. e peak area ratio of a test specimen is applied to the calibration curve to
obtain its pentazocine concentration.
Assessment ... dimethylsilicone stationary phase (in-
termediately polar) can be used, regardless of manufacturers.
b) Any type of GC/MS instruments, to which a capillary column can be attached, can be
used.
c) With a computer ... human plasma by high performance liquid
chromatography. Pharmazie 46:464–465
8) Seno H, Kumazawa T, Ishii A et al. (20 00) Determination of pentazocine in human whole blood and urine by gas...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
Ngày tải lên :
08/11/2013, 01:15
... is rapid and distinct visual hallucination takes place
45 min–1 h a er oral intake of about 20 àg of LSD [1]. e hallucination becomes most marked
2 3 h a er the intake and lasts for 8– 12 h.
In ... Albert Hofmann who did synthesize the compound; the pharmaco-
logical activity can be obtained by oral administration of as small as 20 75 àg of LSD. e ab-
sorption of LSD from the digestive tract ... powerful hallucinogenic
drugs of abuse. LSD was explosively abused in U.S .A. in the latter half of the 1960s. In Japan,
the amount of seizure of LSD is much smaller than that of methamphetamine....
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)
Ngày tải lên :
08/11/2013, 01:15
... 467 :22 7 23 5
24 ) Tsuchihashi H, Nakajima K, Nishikawa M et al. (1991) Determination of methamphetamine and amphetamine
in urine by headspace gas chromatography/mass spectrometry. Anal Sci 7:19 22
... dis-
seminated intravascular coagulation and death [19, 20 ]. A detailed review by Kalant [16] re-
vealed that 87 MDAs-related fatalities were associated with hyperpyrexia, rhabdomyolysis, in-
travascular ...
readily absorbed from the intestinal tract and reaches its peak concentration in plasma about
2 h a er oral administration [21 , 22 ]. e doses of 50, 75 and 125 mg in the usual “recreational”...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)
Ngày tải lên :
08/11/2013, 01:15
... Figure 8 .2
Poisoning case, and toxic and fatal concentrations
A 28 -year-old white man [24 ], who had had a history of drug abuse, exhibited bizarre behav-
ior on an airline ight; he was transferred ... (20 01) Analysis of urine samples in cases of alleged sexual assault: case
history. In: Salamore SJ (ed) Benzodiazepines and GHB: Detection and Pharmacology. Humana Press, Totowa,
pp 127 –144
... MA, Miller ML et al. (20 00) Analysis of biofluids for gamma-hydroxybutyrate (GHB)
and gamma-butyrolactone (GBL) by headspace GC-FID and GC-MS. J Anal Toxicol 24 : 421 – 428
17) Couper FJ, Logan...
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