drugs and poisons in humans a handbook of practical analysis pdf
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)
... transformation in rats. J Pharm Sci 74:780–782 10) Kielbasa WB, Bauer JA, Fung HL (1999) Analysis of isobutyl nitrite inhalant in rat and human blood: application for pharmacokinetic investigations. ... manufacturing drugs or as reagents for synthesis in industries; they are also used as aromatics. Because of their pharmacological e ect, alkyl nitrites are being abused as uncontrolled inhalant drugs ... consisting of the concentration of an alkyl nitrite on the horizontal axis and peak area on the vertical axis. e concentration of the analyte in a specimen is calculated using the calibration curve.Assessment...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)
... For quantitative analysis of DAEMS, various concentrations of DAEMS are spiked into blank serum specimens containing a xed amount of DAEMO (IS) each and extracted as described before. Since ... gradually and carefully. If VX itself remains, there is a danger of the secondary exposure for an analyst; the manipulations including the above evaporation should be done inside a dra chamber.f) ... base peaks of DAEMS and DAEMO (IS) equally appear at m/z 114, the SIM measurements should be made using this single ion to construct a cali-bration curve for DAEMS consisting of peak area ratio...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)
... GC/MS analysis of ∆9-THC-11-oic acid in urine 188 Cannabinoids and their metabolites GC analysis of cannabinoids in plant specimens a Reagents and their preparationã Extraction and puri cation ... CBD, CBN and 5α-cholestane. GC analysis of cannabinoids in plant specimens 192 Cannabinoids and their metabolites e Substance Abuse and Mental Service Administration (SAMSA) in USA set the ... resin of the cannabis plant. Since the main component of cannabis, ∆9-tetrahydrocannabi-nol ( ∆9-THC), has various psychopharmacological e ects including hallucination, the can-nabis and...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
... Matsubara K, Fukushima S, Akane A et al. (1992) Increased urinary morphine, codeine and tetrahydropapavero-line in Parkinsonian patient undergoing L-3,4-dihydroxyphenylalanine therapy: a possible ... Pharmaceutical Society of Japan (ed) (1992) Standard Methods of Chemical Analysis in Poisoning – With Commentary –, 4th edn. Nanzando, Tokyo, pp 230–234 (in Japanese) 200 Morphine and its analogues⊡ ... concentrations 196 Morphine and its analoguesMain metabolic pathways of morphine, heroin and codeine. The thick and thin arrows show the main and minor metabolic pathways, respectively.⊡ Figure...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)
... (1987) Cyanosis in infants caused by nitrates in well water. JAMA 257:2788–2792 12) Fan AM, Steinberg VE (1996) Health implications of nitrate and nitrite in drinking water: an update on methe-moglobinemia ... methemoglobinemia be-comes severe, it causes cyanosis, headache, easy fatigability, respiratory and conciousness dis-turbances and nally death. e fatal methemoglobinemia is rare, but fatal ones a ... was disclosed that he had ingested nitrate. e analytical results for nitrite and nitrate in his blood and stomach contents are shown in > Table 5.2. An example of the gas chromatograms...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)
... 285, 290alternative specimens 9Amanita neoovoidea 480Amanita pantherina 469Amanita phalloides 469Amanita verna 469, 474Amanita virosa 469, 473amanitin 473, 477, 479amido-type local anesthetic ... 137aldicarb 566aldrin 529alkylated adducts 85alkylated DNAs 85alkylation 30alkyl nitrites 153, 655allobarbital 305, 308allylesterase 624allyxycarb 566alminoprofen 325, 330, 332alprazolam ... phenomenon that the absorbance maximum of weakly acidic Met-Hb at 630 nm disappears by addition of cyanide. Met-Hb concentration can be easily determined as the ratios of the absorbance changes in- duced...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)
... for urine sampled 0–1 h a er cocaine inhalation; the ratio was 10.6 on average for urine sampled 0–8 h a er the inhalation. e ratios increased according to the increase in time interval between ... USA, but in Japan the number of such cases is limited. e author et al. experienced a fatal cocaine poisoning case and measured concentrations of cocaine and its metabolites in body uids and ... in blood, a satisfactory mass spectrum can be obtained. For BE, Metabolic pathways of cocaine.⊡ Figure 4.4Toxic and fatal concentrations 212 Cocaine and its metabolites and tablets of 3,4-methylenedioxymethamphetamine...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)
... concentration in the horizontal axis and peak area ratio of pentazocine to IS in the vertical axis. e peak area ratio of a test specimen is applied to the calibration curve to obtain its pentazocine ... Determination of pentazocine in human plasma by high performance liquid chromatography. Pharmazie 46:464–465 8) Seno H, Kumazawa T, Ishii A et al. (2000) Determination of pentazocine in human whole ... cases of pentazocine abuse especially for medical and co-medical workers. e drug is being regulated as a subclass compound of narcotics (DEA class: IV).Pentazocine in both antemortem and postmortem...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
... tract is rapid and distinct visual hallucination takes place 45 min–1 h a er oral intake of about 20 àg of LSD [1]. e hallucination becomes most marked 2–3 h a er the intake and lasts for ... powerful hallucinogenic drugs of abuse. LSD was explosively abused in U.S .A. in the latter half of the 1960s. In Japan, the amount of seizure of LSD is much smaller than that of methamphetamine. ... 8–12 h. In this chapter, a detection method by TLC and con rmatory analysis by GC/MS for LSD are presented.Reagents and their preparation ã LSD can be obtained from each local bureau of drug...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)
... H, Nakajima K, Nishikawa M et al. (1991) Determination of methamphetamine and amphetamine in urine by headspace gas chromatography/mass spectrometry. Anal Sci 7:19–22 25) Shima N, Kamata T, ... per tablet) as the primary ingredient, sometimes smaller amounts of amphetamines and/ or other pharmaceutical agents, such as ca eine and ketamine [4, 5].Structures of MDA and its analogues.⊡ ... intestinal tract and reaches its peak concentration in plasma about 2 h a er oral administration [21, 22]. e doses of 50, 75 and 125 mg in the usual “recreational” range for healthy human...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)
... respectively.-Hydroxybutyric acid 244 Phencyclidine Center. At admission, he stared straight ahead, following commands but not responding verbally; the levels of serum creatinin kinase and aspartate aminotransferase ... Ishii and Yoshinao KatsumataIntroductionPhencyclidine ( PCP) (> Fig. 8.1), a synthetic arylcyclohexylamine hallucinogen, had been rst applied as an anaesthetic to animals and then to humans ... urine samples in cases of alleged sexual assault: case history. In: Salamore SJ (ed) Benzodiazepines and GHB: Detection and Pharmacology. Humana Press, Totowa, pp 127–144 11) Takahara J, Yunoki...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt
... MO, USA). Pure powder of perazine and clospi-razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of upentixol by Takeda Chem. Ind. Ltd., Osaka, Japan; that of thioproperazine by ... Yoshinao KatsumataIntroductionPhenothiazine drugs, including chlorpromazine and levomepromazine, have been being widely used as neuroleptics ( major tranquilizers), antiparkinsonian drugs and ... qualitative and quantitative analysis of phenothiazines in human body uids using useful GC/MS and LC/MS are presented.GC/MS analysis Reagents and their preparationi. ReagentsChlorpromazine, tri...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx
... (ECD). Since, in this chapter, poisoning cases with ingestion of large amounts of drugs are assumed, HPLC analysis with a photodiode array detector can be realized for several ten ng/mL of the drugs. ... 13) Igarashi K, Kasuya F, Abe T et al. (1995) Simultaneous determination of haloperidol and its neurotoxic metabo-lite in plasma and brain tissue from schizophrenic patients treated with haloperidol ... Forensic and Pharmaceutical Chemists. Walter de Gruyter, Berlin, pp 707–718 20) Uges DRA, Conemans JMH (2000) Antidepressants and antiphychotics. In: Bogusz MJ (ed) Handbook of Analytical Separations...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt
... the reuptake of norepinephrine and serotonin and by accerelating the release of them at synaptic terminals of neurons in the brain. As characteristic structures of such drugs showing antidepressive ... tricyclic and tetracyclic antidepressants and carbamazepine obtained by HPLC-UV. A: carbamazepine, B: desipramine, C: maprotiline, D: nortriptyline, E: amoxapine, F: setiptiline, G: mianserin, H: ... by Takeda Chem. Ind. Ltd., Osaka, Japan; dosulepin by Kaken Pharmaceutical Co., Ltd., Tokyo, Japan; lofepramine by Daiichi Pharmaceutical Co., Ltd., Tokyo, Japan; and setip-tiline by Mochida...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 30) doc
... dis-criminate among unchanged, hydroxylated and conjugated forms, and also among similar types of benzodiazepines. LC/MS analysis of triazolam and its metabolitesTo analyze drugs in human specimens ... described. In addition, the LC/MS analysis of triazolam, and its metabolites 4-hydroxy-triazolam and α-hydroxytriazolam is also presented.GC/MS analysis of benzodiazepines in blood and urineReagents ... diazepam, udiazepam, urazepam, prazepam, utoprazepam, dipotassium clorazepate, medazepam, chlordiazepoxide, unitrazepam, alprazolam, midazolam, etizolam and brotizolam for both blood and...
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- strickland and parsons 1968 a practical handbook of seawater analysis
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