Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 31) ppt
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 31) ppt
... Tanaka E, Nakamura T, Nagashima A et al. (2001) Determination of plasma bromvalerylurea and its main meta-bolite by a simple high-performance liquid chromatographic method and quantitation of ... screening of drugs in biological materials by gas chromatography and gas chromatography-mass spectrometry. A fatal poisoning by ingestion of a drug containing acetaminophen, ethenzamide and bromvaleryurea. ... bromide and urea: 5 g of 2-bromohexanoyl bromide (Aldrich, Milwaukee, WI, USA) and an equimolar amount of urea are placed in a 100 mL volume eggplant-shaped glass ask and warmed in a water bath...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt
... MO, USA). Pure powder of perazine and clospi-razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of upentixol by Takeda Chem. Ind. Ltd., Osaka, Japan; that of thioproperazine by ... Springer-Verlag Berlin Heidelberg 2005II.3.1 Phenothiazines by Akira Ishii and Yoshinao KatsumataIntroductionPhenothiazine drugs, including chlorpromazine and levomepromazine, have been being ... available. In this chapter, the methods of qualitative and quantitative analysis of phenothiazines in human body uids using useful GC/MS and LC/MS are presented.GC/MS analysis Reagents and...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx
... timiperone and spiperone with relatively high molecular weights, LC/MS may be most suitable.Poisoning cases, and toxic and fatal concentrations A 2-year plus 5 month-old female and an 11-month-old male ... dyskinesia of the face, appeared. us, diphenhydramine was injected into her intravenously; she recov-ered 4 days a er admission. For the male baby, similar treatments, such as intravenous injec-tion ... bromperidol was used as IS for analysis of haloperidol and vice versa. is is because both drugs are not simultaneously administered in most cases.d) All glasswares, including glass centrifuge...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt
... antidepressants and carbamazepine obtained by HPLC-UV. A: carbamazepine, B: desipramine, C: maprotiline, D: nortriptyline, E: amoxapine, F: setiptiline, G: mianserin, H: imipramine, I: amitriptyline, ... 52:1190–1195 (in Japanese) 3) Tanaka E, Terada M, Nakamura T et al. (1997) Forensic analysis of eleven cyclic antidepressants in human biolo-gical samples using a new reversed-phase chromatographic ... the reuptake of norepinephrine and serotonin and by accerelating the release of them at synaptic terminals of neurons in the brain. As characteristic structures of such drugs showing antidepressive...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 32) ppt
... barbiturateCase 1 [27]: a 40–45 year-old (estimated) female was found dead on a bed of a hotel. In her room, 2 tablets of Vegetamin (a combined drug containing, phenobarbital, promethazine and ... GC and HPLC are presented.Incidence of fatal barbiturate poisoning cases. Since fatal cases due to Vegetamin® tablets containing phenobarbital are many, its incidence rate is also shown in ... methylcyclo-barbital. HPLC analysis [10]Reagents and their preparation• Each barbiturate is dissolved in methanol to prepare 10 µg/mL standard solution and stored at –20 °C.• As internal standard...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 37) pptx
... phenytoin and carbamazepine-epoxide can be purchased from Sigma. Lamotrigine, carbamazepine-diol and 9-hydroxy-methyl-10-carbamyl acridan were reported to be obtainable from Chiba-Geigy (Basel, ... preparation• Carbamazepine, ethosuximide, phenytoin, primidone, phenobarbital, diazepam, oxaze-pam, nitrazepam and 5-( 4-methylphenyl )-5 -phenylhydantoin (internal standard, IS) can be all purchased from ... carbamazepine) and two carbamazepine metabolites ( carbamazepine-diol and carbamazepine- epoxide) can be detected from human plasma (> Figure 5.3). e detec-tion limits of each drug was about...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 38) pptx
... uoroacetic acid can be added to a mobile phase as an ion-pairing reagent for analysis of the quaternary amino muscle relaxants [6].e) For solid-phase extraction of the drugs, weak cation-exchanger ... Dragendorff reagent; ➄: iodoplatinate reagentTLC analysis 362 Muscle relaxants Direct inlet MS analysis [4]Reagents and their preparation• A 1-g aliquot of iodine and 2 g potassium iodide are dissolved ... peripheral-acting muscle relaxants are intentional and/ or homicidal. In this chapter, therefore, analytical methods only for the peripheral-acting muscle relaxants (> Table 6.2) are dealt with....
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 39) ppt
... β-receptors; they cause hypotension by decreasing the heart beat rate and cardiac output, and prevent the attacks of arrhythmia and angina pectoris. In the brain, the drugs attenuate migraine ... e β-blockers are structurally classi ed into isopropylamino drugs such as propranolol and tertiary butylamino drugs such as nadolol; and many products containing 26 kinds of β-blockers are ... due to a TFA derivative of a β-blocker can be obtained a er heating and evaporation of the excess reagent; for example, the mass spectrum of nadolol-tris-O-TMS gives the base peak at m/z 86,...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 43) pptx
... for bleaching and other purposes. Sodium hypochlorite ( NaClO) aqueous solu-tion is usually used as a disinfectant, bleaching agent, fungicide and ink eraser, and is thus usually included in detergents ... solutions are analyzed by the above CE to construct a calibration curve (concentration of a hypochlorite ion in a specimen vs. peak area). A peak area obtained from a specimen is applied to the calibration ... detergents for laundry. Calcium hypochlorite [ Ca(ClO)2, bleaching pow-der] is also used as a bleaching agent and disinfectant. e kinds of household utensils contain-ing hypochlorite are numerous;...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 46) pptx
... the author et al. [1] experienced an actual case of ingestion of a large amount of permethrin-containing emulsion (Adio®, Agros, Tokyo, Japan) and measured the concentrations of its cis and ... pretreatments and rapidness of analysis; it seems more useful than GC in clinical analysis. HPLC chromatograms for extracts of sera obtained from a permethrin-poisoned patient 3 h and 3 months after ... metabolic acidosis and renal dysfunction. By treatments, such as endotra-cheal intubation, gastrolavage, administrations of activated charcoal and magnesium citrate and transfusion, his conditions...
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