Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
... rapid and distinct visual hallucination takes place 45 min–1 h a er oral intake of about 20 µg of LSD [1]. e hallucination becomes most marked 2–3 h a er the intake and lasts for 8–12 h. In ... LSD is rapidly metabolized in human bodies. As metabolites of LSD, 2-oxo-LSD, 3-, 1 3- and 14-hydroxy-LSDs and an N-de-ethyl-LSD are known [3]. A er oral ingestion of 160 µg LSD, the maximum blood ... Japan (ed) (1992) Standard Methods of Chemical Analysis in Poisoning – With Commentary –. Nanzando, Tokyo, p 43 and p 151 (in Japanese) 3) Cody JT (2000) Hallucinogens. In: Bogusz MJ (ed) Handbook...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)
... are also used as aromatics. Because of their pharmacological e ect, alkyl nitrites are being abused as uncontrolled inhalant drugs and causing a social problem [4]. Although there are many reports ... headspace (HS)-gas chromatography (GC) and liquid-liquid extraction-GC are presented. Determination of isobutyl nitrite in aqueous solution by headspace-GC Reagents and their preparation • A ... specimen). In principle, the sampling, extraction and GC analysis should be made at low temperature, in a gastight state and in a short time. is method is applicable to other biomedical specimens and...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)
... concentrations of DAEMS are spiked into blank serum specimens containing a xed amount of DAEMO (IS) each and extracted as described before. Since the base peaks of DAEMS and DAEMO (IS) equally appear ... biofluids by gas chromatography-mass spectrometry and liquid- liquid-solid phase-transfer-catalyzed pentafluorobenzylation. J Anal Toxicol 23:86–93 11) Black RM, Read RW (1998) Analysis of degradation ... chromatogram (TIC) and a mass chromato- gram; (b) an EI mass spectrum of DAEMS; (c) a CI mass spectrum of DAEMS. ⊡ Figure 2.2 623VX and its decomposition products data of animals. According to...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)
... EI mass spectra of ∆ 9 -THC, CBD, CBN and 5α-cholestane. GC analysis of cannabinoids in plant specimens 190 Cannabinoids and their metabolites GC/MS analysis of ∆ 9 -THC-11-oic acid in urine ... resin of the cannabis plant. Since the main component of cannabis, ∆ 9 -tetrahydrocannabi- nol ( ∆ 9 -THC), has various psychopharmacological e ects including hallucination, the can- nabis and ... analysis of ∆ 9 -THC-11-oic acid in urine 192 Cannabinoids and their metabolites e Substance Abuse and Mental Service Administration (SAMSA) in USA set the cuto value of ∆ 9 -THC-11-oic acid in...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
... 8) Matsubara K, Fukushima S, Akane A et al. (1992) Increased urinary morphine, codeine and tetrahydropapavero- line in Parkinsonian patient undergoing L-3,4-dihydroxyphenylalanine therapy: a possible ... patient, several grams of an opiate do occasionally not cause death. Toxic and fatal concentrations 204 Morphine and its analogues As a result of analysis of 203 fatal cases with morphine and ... Qualitative analysis is made by the comparison of the retention time of a peak of a specimen with that of the authentic standard and also by the con rmation of the absence of such a peak in a...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)
... methemoglobinemia be- comes severe, it causes cyanosis, headache, easy fatigability, respiratory and conciousness dis- turbances and nally death. e fatal methemoglobinemia is rare, but fatal ones a ... Various known amounts of nitrate and a xed amount of IS are added to blank specimens and processed in the same way to construct a calibration curve. e peak area ratio of nitrate to IS obtained ... that he had ingested nitrate. e analytical results for nitrite and nitrate in his blood and stomach contents are shown in > Table 5.2. An example of the gas chromatograms in the present case...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)
... pantherina 469 Amanita phalloides 469 Amanita verna 469, 474 Amanita virosa 469, 473 amanitin 473, 477, 479 amido-type local anesthetic 385 1-amino- 4- phenylbutane 173 2-amino-6-hydroxymethyl- 8-hydroxyquinazoline ... 165 N-methyl- 1-( 3,4-methylene- dioxyphenyl )-2 -butan- amine 229 N-methyl- 1-( 3,4-methylene- dioxyphenyl )-3 -butan- amine 233 N-methyl-bis(tri uoro- acetamide) 371 N-methyl-N-(trimethylsilyl )- tri ... N-(phosphonomethyl )- β-alanine 555 N-acetyl-p-phenylene- diamine 415 N-allylcarbamate herbicides 559 n-butylbenzene 159 N-chloromethylphthalimide 327 N-de-ethyl-LSD 228 n-decane 165 n-heptane 165 n-hexane 165...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)
... e author et al. experienced a fatal cocaine poisoning case and measured concentrations of cocaine and its metabolites in body uids and various organs. A 41-year-old male was found dead in a ... suggesting a relatively short period between the times of his ingestion and death. In addi- tion, the ratios of cocaine to BE in blood and in the brain, and the brain-to-blood ratios of cocaine and ... postmortem interval (period between death and autopsy) and the in vitro interval (period between sampling and analysis) are variable; the hydrolytic rate of cocaine shows great variation. Usually,...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)
... composed of pen- 221 tazocine concentration in the horizontal axis and peak area ratio of pentazocine to IS in the vertical axis. e peak area ratio of a test specimen is applied to the calibration ... commercially avail- able. ii. Preparation • Pentazocine and dextromethorphan solutions: the drugs are separately dissolved in appro- priate amount of methanol; a 10–20 µL aliquot was added to 1 mL of whole ... obtain its pentazocine concentration. Assessment of the method > Table 5.1 shows EI mass spectra of pentazocine and IS. e base peaks unfortunately appeared in a low mass range at m/z 70 and...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)
... LC/MS analyses of MDAs in the forms of tablets and those for GC/MS analysis of MDAs and their main metabolites 4-hydroxy-3-me- thoxymethamphetamine ( HMMA) and 4-hydroxy-3-methoxyamphetamine ( HMA) ... simultaneou determination of amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine, 3,4-methylenedioxymethamphetamine, and 3,4-methylenedioxyethyl- amphe tamine in urine by solid-phase extraction ... metabolic pathway of MDMA in humans is the 3,4-Methylenedioxyamphetamines 234 3,4-Methylene dioxyamphetamines Mass spectra of TFA derivatives of MDA, MDMA, MDEA, MBDB and HMDMA obtained by GC/MS....
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